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Iron complexes, [Fe(NCCH3)6][cis-Fe(InX3)2(CO)4] (X = Cl: , Br: , I: ) containing two terminal indium fragments, were synthesized. Their structures were determined using X-ray analysis. The bonding mode of the Fe-In bonds in the anionic part was investigated using (57)Fe Mössbauer and IR spectroscopy. These complexes represent the first example of transition metal complexes containing two terminal indium fragments.

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Synthesis and characterization of [Fe(NCCH3)6][cis-Fe(InX3)2(CO)4] (X = Cl, Br, I) containing two terminal indium fragments