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The polydentate ligand Bis–tris propane is used to assemble two Cu/Zn heterometallic complexes: a tetramer which displays an unusually strong Cu( ii )⋯Cu( ii ) exchange given the Cu⋯Cu separation or, in the presence of base, a hexadecanuclear complex with a remarkable double-concentric ring structure.

Directed synthesis of {CuII2ZnII2} and {CuII8ZnII8} heterometallic complexes