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M'0.2Mn0.8PS3·0.25H2O materials are obtained by a mild microwave assisted reaction (M' = Co(II), Ni(II), Cu(II), Zn(II)), which permitted us to obtain the first copper(ii) bimetallic phase. All these materials have a lower energy gap and antiferromagnetic interactions with lower values of the Weiss constant, than that of the pristine phase MnPS3.

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First copper(<scp>ii</scp>) phase M′0.2Mn0.8PS3·0.25H2O and analogous M′ = CoII, NiII and ZnII materials obtained by microwave assisted synthesis

First copper(ii) phase M′0.2Mn0.8PS3·0.25H2O and analogous M′ = CoII, NiII and ZnII materials obtained by microwave assisted synthesis

First copper(ii) phase M′0.2Mn_0.8PS₃·0.25H₂O and analogous M′ = Co^II, Ni^II and Zn^II materials obtained by microwave assisted synthesis