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Graphitic-C3N4 is shown for the first time to catalyse photoacetalization of aldehydes/ketones with alcohols to acetals in high yields using visible light under ambient conditions; transient charge separation over the material is effective to catalyse the reaction in the absence of Lewis or Brønsted acids, giving a new green alternative catalyst.

Graphitic carbon nitride catalysed photoacetalization of aldehydes/ketones under ambient conditions