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The first example of a triply cyclometalated homopolynuclear tri-Ir(III) complex with additional carbene donors is presented. Cooperative catalysis and the interplay between homogenous and heterogeneous catalyses are discussed for the tri-Ir(III) complex and a related non-cyclometalated tri-Pd(II) complex.

Triply cyclometalated trinuclear iridium(iii) and trinuclear palladium(ii) complexes with a tri-mesoionic carbene ligand