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Treatment of anhydrous FeCl2 with 2 equiv. of the pincer ligand PNP-Ph afforded the diamagnetic cationic octahedral complex [Fe(κ(3)-P,N,P-PNP)(κ(2)-P,N-PNP)Cl](+) featuring a κ(2)-P,N-bound PNP ligand. Preliminary reactivity studies revealed that the κ(2)-P,N-bound PNP ligand is labile reacting with CO to afford trans-[Fe(PNP-Ph)(CO)2Cl](+).

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An iron(<scp>ii</scp>) complex featuring κ3 and labile κ2-bound PNP pincer ligands – striking differences between CH2 and NH spacers

An iron(ii) complex featuring κ3 and labile κ2-bound PNP pincer ligands – striking differences between CH2 and NH spacers

An iron(ii) complex featuring κ³ and labile κ²-bound PNP pincer ligands – striking differences between CH₂ and NH spacers