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The use of the novel pro-ligand H4L combining the complimentary phenolic oxime and diethanolamine moieties in one organic framework, results in the formation of the first example of a [Mn(III)12] truncated tetrahedron and an extremely rare example of a Mn cage conforming to an Archimedean solid.

A truncated [MnIII12] tetrahedron from oxime-based [MnIII3O] building blocks

A truncated [Mn^III₁₂] tetrahedron from oxime-based [Mn^III₃O] building blocks