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The immobilisation of electrocatalysts for CO2 reduction onto light harvesting semiconductors is proposed to be an important step towards developing more efficient CO2 reduction photoelectrodes. Here, we report a low cost nickel cyclam complex covalently anchored to a metal oxide surface. Using transient spectroscopy we validate the role of surface immobilisation on enhancing the rate of photoelectron transfer. Furthermore [Ni(1,4,8,11-tetraazacyclotetradecane-6-carboxylic acid)](2+) (2) is shown to be a very active electrocatalyst in solution.

physical chemistry chemical physics/pccp. physical chemistry chemical physics

A functionalised nickel cyclam catalyst for CO<sub>2</sub> reduction: electrocatalysis, semiconductor surface immobilisation and light-driven electron transfer

A functionalised nickel cyclam catalyst for CO2 reduction: electrocatalysis, semiconductor surface immobilisation and light-driven electron transfer

A functionalised nickel cyclam catalyst for CO₂ reduction: electrocatalysis, semiconductor surface immobilisation and light-driven electron transfer