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A series of paramagnetic di(aryl)alkynylphosphine oxides [PF6] featuring an open-shell [Fe(κ(2)-dppe)(η(5)-C5Me5)](+) endgroup were obtained by oxidation of their neutral Fe(II) parents 3a-c, themselves obtained in a simple and nearly quantitative fashion from the corresponding Fe(II) metallophosphines 1a-c. The new organometallic radicals were characterised by NMR and ESR and were shown to be perfectly stable in solution, in contrast to species such as 1a-b[PF6] which readily dimerise.

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Easy and quantitative access to Fe(<scp>ii</scp>) and Fe(<scp>iii</scp>) di(aryl)alkynylphosphine oxides featuring [Fe(dppe)Cp*] endgroups: terminal PO functionality blocks the dimerisation of the Fe(<scp>iii</scp>) derivatives

Easy and quantitative access to Fe(ii) and Fe(iii) di(aryl)alkynylphosphine oxides featuring [Fe(dppe)Cp*] endgroups: terminal PO functionality blocks the dimerisation of the Fe(iii) derivatives