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Unexpected panelling by μ6-CO3(2-) anions has been observed to support the formation of a new and unusual Co15 cluster. The arrangement is further stabilised by bis-phenolate ligands which assemble in a manner akin to tetrahomodioxacalix[4]arene. The reaction proceeds in very low yield as μ6-CO3(2-) anions are formed in situ, but targeted synthesis by addition of carbonate improves synthetic yield and highlights the pivotal role of this anion in the overall assembly process.

Discovering the pivotal role of carbonate in the formation of a bis-phenolate supported Co15cluster

Discovering the pivotal role of carbonate in the formation of a bis-phenolate supported Co₁₅cluster