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The structure of an unusual dimerisation mode of a triphenylimidazolyl radical has been elucidated, revealing a relatively long C–C bond. The diffraction-quality single crystals were produced under continuous irradiation by photocrystallisation in an adaption of the method that should be widely applicable to other photochromic systems

Photocrystallisation of the 2C–2′C dimer of a triphenylimidazolyl radical