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Ligand metathesis, Co(II) coordination, and partial condensation reactions of an archetypal {Zr6} zirconium oxocarboxylate cluster result in the first example of the coexistence of the distinct zirconium oxide frameworks {Zr6O8} and {Zr12O22}. Even minor modifications to the reaction conditions push this apparent equilibrium towards the {Zr6O8}-based product.

Solid-state coexistence of {Zr12} and {Zr6} zirconium oxocarboxylate clusters

Solid-state coexistence of {Zr₁₂} and {Zr₆} zirconium oxocarboxylate clusters