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The reaction of 4,5-dicyano-2-methoxyimidazole (L1) with Co(NO3)2·6H2O under solvothermal conditions in DMF, a MOF, and a hydrogen-bonded network consisting of tetradecanuclear Co(ii)14-metal organic cube () are achieved. shows the bcu net with 14 cobalt atoms.

chemical communications

A supramolecular Co(<scp>ii</scp>)<sub>14</sub>-metal–organic cube in a hydrogen-bonded network and a Co(<scp>ii</scp>)–organic framework with a flexible methoxy substituent

A supramolecular Co(ii)14-metal–organic cube in a hydrogen-bonded network and a Co(ii)–organic framework with a flexible methoxy substituent

A supramolecular Co(ii)₁₄-metal–organic cube in a hydrogen-bonded network and a Co(ii)–organic framework with a flexible methoxy substituent