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A highly diastereoselective formal [3+2+1]-cycloaddition reaction that produces multi-functionalized bicyclic pyrazolidinone derivatives is achieved in moderate to high yield by Rh2(4S-MPPIM)4-catalyzed reaction of azomethine imines with two molecules of a diazo ketone.

Dirhodium(ii)-catalyzed formal [3+2+1]-annulation of azomethine imines with two molecules of a diazo ketone