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A new hybrid organic–inorganic non-linear optical crystalline material, L-argininium perrhenate hasbeen synthesized. The crystal belongs to P212121 space group, has a good optical quality and hightransmission in the visible and near infra-red spectral regions. L-argininium perrhenate has highbirefringence and is more than four times as efficient as KDP in second harmonic generation, making ita potentially attractive material for non-linear optical applicationsThis work was financially supported by the European Regional Development Fund (ERDF) through Programa Operacional Factores de Competitividade (COMPETE: FCOMP-01-0124-FEDER-014628) and the Portugal Fundacao para a Ciencia e Tecnologia (PTDC/CTM-NAN/114269/2009, PTDC/CTM/105597/2008 and Pest-C/FIS/UI0036/2011)

Synthesis, structure and non-linear optical properties of l-argininium perrhenate crystal