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The porous organosilica framework containing Troger's base (TB) prepared by mild sol–gel synthesis from 2,8-bis-silylated TB precursor contains a mixture of two point attached TB and one point attached TB units, resulting from unexpected partial Si–C bond cleavage as demonstrated by 29Si MAS NMR spectroscopy and by selective chemo-desorption of the anchored organic part of the hybrid material.

Si–C attachment points during sol–gel synthesis of organosilicas from 2,8-bis-silylated Tröger's base as building block precursor