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The synthesis procedure for isomeric periodic mesoporous organosilicas with E-configured ethenylenebridges was investigated using the homemade pure E-isomer of 1,2-bis(triethoxysilyl)ethene. The pH,aging temperature and the presence of cosolvents played a key role in obtaining well-orderedmesoporous materials with controllable properties and morphologies. By fine-tuning the reactionmixture acidity, PMOs with high surface areas and pore volumes could be attained. By selecting variousalcohols as cosolvents and optimizing the alcohol concentration, PMOs with crystal-like disc shaped,fibrous and spherical particle morphologies were obtained. The synthesis temperature of theseethenylene-bridged PMOs influences the pore size, structure, connectivity and volume

Isomeric periodic mesoporous organosilicas with controllable properties