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A nickel-catalyzed [2+2+2] cycloaddition of two molecules of aryne and an alkene moiety in a alpha,omega-diene afforded 9,10-dihydrophenanthrene derivatives in good yields.

Nickel-catalyzed [2 + 2 + 2] cycloaddition of arynes and an unactivated alkene: synthesis of 9,10-dihydrophenanthrene derivatives