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6 pages, 6 figures, 2 tables.Micro- and sub-micro particles of complex [Mn12O12(O2CC6H5)16(H2O)4] ( 1) with controlled size and polymorphism have been prepared by dense-gas crystallization techniques, showing a remarkable particle size influence on the magnetization relaxation rates.This work was supported by DGI (Spain) under projects\udMAT2002-0043 and MAT2003-04699 and by the European\udCommission under the NoE MAGMANET (Contract NMP3-\udCT-2005-515767) and QUEMOLNA Marie Curie RTN\ud(Contract MRTN-CT-2003-5044880). Javier Campo and Nora\udVentosa thank the Ramon y Cajal Program of Ministerio de\udEducación y Tecnología (Spain) for their contracts. Maria\udMuntó thanks the Consejo Superior de Investigaciones\udCientíficas (CSIC) for her PhD bursary and Jordi Gómez-\udSegura thanks the European Community for his PhD grant.Peer reviewe

Controlled crystallization of Mn12single-molecule magnets by compressed CO2and its influence on the magnetization relaxation

Controlled crystallization of Mn₁₂single-molecule magnets by compressed CO₂and its influence on the magnetization relaxation