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Novel lanthanum(III), europium(III) and terbium(III) compounds of a benzo-15-crown-5 [60]fulleropyrrolidinewere isolated in the solid state and characterised using vibrational (infrared and Raman) spectroscopy andby 13C CP MAS NMR for the lanthanum(III) compound. The photoluminescence properties wereinvestigated for the europium(III) and terbium(III) compounds. The related [Tb(H2O)3(NO3)2(acac)]  C14H20O5 [where acac  ¼ acetylacetonate and C14H20O5 ¼ benzo-15-crown-5] supramolecular adduct wasisolated using similar synthetic conditions, in the absence of [60]fullerene, and its crystal structure used as amodel for the coordination sphere of the lanthanide [60]fullerene derivatives, with further supportingevidence given by photoluminescence measurements

new journal of chemistry

Lanthanide compounds containing a benzo-15-crown-5 derivatised [60]fullerene and the related [Tb(H2O)3(NO3)2(acac)]·C14H20O5supramolecular adduct