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A 2D grid-shaped cyanide-bridged Co(II)-Au(I) bimetallic coordination polymer, [Co(DMF)2(Au(CN)2)2], has been prepared from the [Au(CN)2]- building block; sheets associate pair-wise by aurophilic interactions and the compound exhibits zeolite-like properties.

Aurophilicity as a cofactor in crystal engineering. Dicyanoaurate(i) anion as a building block in a novel Co(ii)–Au(i) bimetallic assembly