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Black brookite TiO 2  single-crystalline nanosheets with outstanding photocatalytic activity toward CO 2  reduction is prepared by a facile oxidation-based hydrothermal reaction method combined with post-annealing treatment. Large amount of Ti 3+  defects are introduced into the bulk of brookite nanoparticles, which increases the solar energy absorption and enhances the photocatalytic activity.

Ti3+-self doped brookite TiO2 single-crystalline nanosheets with high solar absorption and excellent photocatalytic CO2 reduction