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Hierarchical TiO 2  micron spheres assembled by nano-plates were prepared through a facile hydrothermal route. Chemical tuning of the TiO 2  through hydrogen reduction (H-TiO 2 ) is shown to increase oxygen-vacancy density and thereby modifies the electronic properties. H-TiO 2  spheres with a polar surface serve as the surface-bound intermediates for strong polysulfides binding. Under the restricting and recapturing effect, the sulfur cathode could deliver a high reversible capacity of 928.1 mA h g −1  after 50 charge-discharge cycles at a current density of 200 mA g −1 . The H-TiO 2  additive developed here is practical for restricting and recapturing the polysulfide from the electrolyte.

Hierarchical TiO2 spheres as highly efficient polysulfide host for lithium-sulfur batteries