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r-BN nanoflakes were synthesized using KBH 4  and NH 4 Cl as the main raw material in a high-purity nitrogen atmosphere. The effects of salt and salt-free conditions and heating temperature on the synthesis of BN were studied. The molten-salt method was used to synthesize BN at 650 °C, which was 250 °C lower than the BN synthesis method without salt. Furthermore, at 1000 °C the prepared flake-like BN crystals showed good crystallinity, uniform morphology, a particle diameter of 200–300 nm, and a thickness of 40–70 nm. Moreover, the specific surface area of BN was 294.26 m 2 /g. In addition, the BN synthesized at 1100 °C had a large elastic modulus value and good oxidation resistance.

Low temperature synthesis via molten-salt method of r-BN nanoflakes, and their properties