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A liquid flow-type electrolyser that continuously produces an alcohol from a carboxylic acid was constructed by employing a polymer electrolyte, named a polymer electrolyte alcohol electrosynthesis cell (PEAEC). Glycolic acid (GC, an alcoholic compound) is generated on anatase TiO 2  catalysts via four-electron reduction of oxalic acid (OX, a divalent carboxylic acid), accompanied with water oxidation, which achieves continuous electric power storage in easily stored GC. Porous anatase TiO 2  directly grown on Ti mesh (TiO 2 /Ti-M) or Ti felt (TiO 2 /Ti-F) was newly fabricated as a cathode having favourable substrate diffusivity. A membrane-electrode assembly composed of the TiO 2 /Ti-M, Nafion 117, and an IrO 2  supported on a gas-diffusion carbon electrode (IrO 2 /C) was applied to the PEAEC. We achieved a maximum energy conversion efficiency of 49.6% and a continuous 99.8% conversion of 1 M OX, which is an almost saturated aqueous solution at room temperature.

scientific reports

Electrochemical Production of Glycolic Acid from Oxalic Acid Using a Polymer Electrolyte Alcohol Electrosynthesis Cell Containing a Porous TiO2 Catalyst