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In this work, we developed a new method for the transformation of organostannanes via radical process. In this reaction, highly reactive carbon radical species can be efficiently generated through HBr-catalyzed photocleavage of C-Sn bond via single electron transfer process. Under aerobic conditions, the  in situ  formed primary/secondary alkyl radicals can be further highly selectively oxidized into carboxylic acids/ketones, respectively.

Transformation of Organostannanes Based on Photocleavage of C-Sn Bond via Single Electron Transfer Process