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A study was conducted to gather information regarding the structural relaxation that occurred in spin-cast, glassy polymer thin films. Two poly(butyl methacrylate) polymers were used to conduct the investigations. These isomers had a large difference in their T g values, whereas elemental compositions of their repeat unit were identical and differences in interactions with solvent or silicon substrate were not expected to affect the experiments. The substrates were single-crystal silicon wafers and used as received, such that the native oxide was on the surface. Films were aged at room temperature under vacuum for different periods up to 24 hours to allow the solvent to leave the film and for the structures to relax.SCOPUS: ar.jinfo:eu-repo/semantics/publishe

Some insights into the structural relaxation of spin-cast, glassy polymer thin films