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The reaction between [Re 2 (μ-H) 2 (CO) 8 ] and [Pt(PPh 3 ) 2 (C 2 H 4 )] at 273 K results in the insertion of the [Pt(PPh 3 ) 2 ] fragment into a Re(μ-H)Re bond, giving the triangular cluster [Re 2 Pt(μ-H) 2 (CO) 8 (PPh 3 ) 2 ], characterized spectroscopically. On increasing the temperature, an irreversible transformation occurs, due to the exchange of one phosphine and one carbonyl between platinum and rhenium. Two other isomers are formed in this way, characterized by 1 H and 31 P NMR, which differ in the location of the phosphine bound to rhenium

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Mixed-metal rhenium-platinum cluster compounds. Synthesis and characterization of three isomers of the triangular cluster complex [Re2Pt(.mu.-H)2(CO)8(PPh3)2]