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All reactions were performed in a drybox or using Schlenk technique under a nitrogen atmosphere with magnetic stirring. Column chromatography was performed with Ultra Pure Silica Gel (SILICYCLE, pH 7.0, 40-63 μm, 60Å). 1H NMR spectra were recorded on a Varian Mercury400 (400.44 MHz) spectrometer. 13C NMR spectra were recorded on a Varian GEMINI-2000 (75.45 MHz), JEOL JNM-A500 (125.65 MHz), or JEOL ECA-600 (150.92 MHz) spectrometers. Chemical shifts were reported in ppm downfield from tetramethylsilane. Elemental analyses were performed by Elemental Analysis Center of Kyoto University. High resolution mass spectra were recorded on a JEOL JMS-700 spectrometer.

The Asymmetric Silaboration of Terminal Allenes Bearing -Stereogenic Centers: Stereoselection Based on Reagent Control