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[reaction: see text] The protiodesilylation of unactivated C(sp3)-SiMe2Ph bonds proceeds efficiently by treatment with tetrabutylammonium fluoride in wet DMF or THF via isolable dimethylsilanol intermediates.

Efficient Protiodesilylation of Unactivated C(sp3)−SiMe2Ph Bonds Using Tetrabutylammonium Fluoride

Efficient Protiodesilylation of Unactivated C(sp³)−SiMe₂Ph Bonds Using Tetrabutylammonium Fluoride