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New spiro-compounds basis of isoquinoline-1,3-dione were prepared by microwave-assisted 1,3-dipolar cycloaddition reactions with azomethine ylides. The reactions performed under microwaves were compared with the same reactions conducted under the classical conditions of thermal heating.

MICROWAVE-ASSISTED [ 3 + 2 ] CYCLOADDITIONS OF AZOMETHINE YLIDES WITH ( E )-4-ARYLIDENE-N-PHENYL-( 2 H )-ISOQUINOLINE-1 , 3-DIONE