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rotational echo double resonance (REDOR) experiments were used to determine homonuclear and heteronuclear interactions that can reflect the intermediate-range order. It was found that the local bonding environments of the L2B crystal and glass are quite similar, whereas there are significant differences in the N2B system. Moreover, the experimental results indicated that the second moment (M2) values of both homo- and heterodipolar interactions measured for the L2B glass are very close to those of its isochemical crystal, in contrast, the M2 values for N2B glass differ significantly from those of its crystal phase. These observations indicate the existence of a strong correlation between structural similarity at both the short and intermediate length scale, and nucleation mechanism.

the journal of physical chemistry c

Structural Similarity on Multiple Length Scales and Its Relation to Devitrification Mechanism: A Solid-State NMR Study of Alkali Diborate Glasses and Crystals