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An electrochemical method for the simultaneous determination of the diffusion coefficient and efficiency of release of probe species from thermoresponsive gels due to their volume phase transition is presented. The method combines steady-state voltammetry at microelectrodes and conductometry, and it is designed for charged redox species. This method might be modified for uncharged systems; in this case instead of the conductometric measurement an additional independent voltammetric experiment in the solution is required. The approach presented here has been examined for positively and negatively charged and uncharged ferrocene

Efficiency of Solute Release from Thermoresponsive Poly(N-isopropylacrylamide) Gels: Electrochemical Studies