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Orthorhombic V 2 O 5 nanowires were successfully synthesized via a hydrothermal method. A cell-configuration system was built utilizing V 2 O 5 as the cathode and 1 M Mg(ClO 4 ) 2 electrolyte within acetonitrile, together with Mg x Mo 6 S 8 ( x ≈ 2) as the anode to investigate the structural evolution and oxidation state and local structural changes of V 2 O 5 . The V 2 O 5 nanowires deliver an initial discharge/charge capacity of 103 mAh g -1 /110 mAh g -1 and the highest discharge capacity of 130 mAh g -1 in the sixth cycle at C/20 rate in the cell-configuration system. In operando synchrotron diffraction and in operando X-ray absorption spectroscopy together with ex situ Raman and X-ray photoelectron spectroscopy reveal the reversibility of magnesium insertion/extraction and provide information on the crystal structure evolution and changes of the oxidation states during cycling.

journal of the american chemical society

In Operando Synchrotron Diffraction and in Operando X-ray Absorption Spectroscopy Investigations of Orthorhombic V2O5 Nanowires as Cathode Materials for Mg-Ion Batteries