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Here we demonstrate the delicate design and construction of hierarchical Co 9 S 8 @ZnIn 2 S 4 heterostructured cages as an efficient photocatalyst for hydrogen evolution with visible light. Two photoactive sulfide semiconductors are rationally integrated into a hierarchical hollow structure with strongly coupled heterogeneous shells and two-dimensional ultrathin subunits. The unique architecture can efficiently facilitate the separation and transfer of light-induced charges, offer large surface area, and expose rich active sites for photocatalytic redox reactions. Owing to the distinctive structural and compositional benefits, the hierarchical Co 9 S 8 @ZnIn 2 S 4 hollow heterostructures without using any cocatalysts show remarkable activity with a hydrogen-producing rate of 6250 μmol h -1 g -1 and high stability for photocatalytic water splitting.

journal of the american chemical society

Formation of Hierarchical Co9S8@ZnIn2S4 Heterostructured Cages as an Efficient Photocatalyst for Hydrogen Evolution