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We demonstrate the rational design and construction of sandwich-like ZnIn 2 S 4 -In 2 O 3 hierarchical tubular heterostructures by growing ZnIn 2 S 4 nanosheets on both inner and outer surfaces of In 2 O 3 microtubes as photocatalysts for efficient CO 2 photoreduction. The unique design integrates In 2 O 3 and ZnIn 2 S 4 into hierarchical one-dimensional (1D) open architectures with double-heterojunction shells and ultrathin two-dimensional (2D) nanosheet subunits. This design accelerates the separation and transfer of photogenerated charges, offers large surface area for CO 2 adsorption, and exposes abundant active sites for surface catalysis. Benefiting from the structural and compositional merits, the optimized ZnIn 2 S 4 -In 2 O 3 photocatalyst exhibits outstanding performance for reductive CO 2 deoxygenation with considerable CO generation rate (3075 μmol h -1 g -1 ) and high stability.

journal of the american chemical society

Construction of ZnIn2S4–In2O3 Hierarchical Tubular Heterostructures for Efficient CO2 Photoreduction