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Incorporation of two 9-borabicyclo[3.3.1]nonyl substituents within the secondary coordination sphere of a pincer-based Fe(II) complex provides Lewis acidic sites capable of binding 1 or 2 equiv of N 2 H 4 . Reduction of the 1:1 Fe:N 2 H 4 species affords a rare Fe(NH 2 ) 2 complex in which the amido ligands are stabilized through interactions with the appended boranes. The NH 2 units can be released as NH 3 upon protonation and exchanged with exogenous N 2 H 4 .

Hydrazine Capture and N–N Bond Cleavage at Iron Enabled by Flexible Appended Lewis Acids