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Conformationally disordered poly{3,4-di[(S)-2-methylbutoxy]thiophene} is prepd. via monomer polymn. by anhyd. FeCl3. Optically active ordered polymer is prepd. by cooling of the polymer to -30 Deg. In the aggregated phases a splitting of the excited state into two exciton levels occurs

Circular Dichroism and Circular Polarization of Photoluminescence of Highly Ordered Poly{3,4-di[(S)-2-methylbutoxy]thiophene}