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The indium sesquisulfide phase is shown by x-ray diffraction and mass spectrometer meast~rements to have a wide solution range at 600 to 800°C. · The existence of InS and In 5 s 6 (here identified as InSl. 12 ) is confirmed and the existen::e of In 3 s 4 is disproved. Mass spectrometer intensities vs time for In 2S+ and s; are used to obtain values of the partiai pressures of In 2S(g) and s2{g) as functions of composition in the range from InS(s) to InSl. 5 (s). At 600 to 800° C the heat of formation of the indium sesquisulfide phase from liquid indium and s2 gas is 0. 37y 44. 3 kcal/ gat.; where y is the at. o/o In, and the corresponding heat of formation of InSJ.. 12 is -27.7kcal/gat. and of.InS is -26.5kcal/gat.

Thermodynamic Stabilities as a Function of Composition for Indium Sulfide Phases from Mass Spectrometer Intensity vs. Time Data1

Thermodynamic Stabilities as a Function of Composition for Indium Sulfide Phases from Mass Spectrometer Intensity vs. Time Data¹