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We demonstrate the existence of discrete single molecular [Mo(132)] Keplerate-type clusters in aqueous solution. Starting from a discrete spherical [Mo(132)] cluster, the formation of an open-basket-type [Mo(116)] defect structure is shown for the first time in solution using analytical ultracentrifugation sedimentation velocity experiments.

Direct Evidence on the Existence of [Mo132] Keplerate-Type Species in Aqueous Solution

Direct Evidence on the Existence of [Mo₁₃₂] Keplerate-Type Species in Aqueous Solution