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The synthesis of a novel ligand system (1) composed of two bipyridine units linked by a crown ether moiety is described. Addition of 2 equiv of (Cu(MeCN) 4 ]BF 4 to 1 and subsequent oxidation yield a dinuclear μ-hydroxo-bridged copper(II) complex, [(1)Cu 2 (OH) 2 BF 4 ]BF 4 .2H 2 O (2). The structure of this complex has been determined by X-ray crystallographic methods

Structure determination, spectroscopic characterization, and magnetic properties of a novel dinuclear copper(II) crown ether bipyridine complex