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The crystal architecture and magnetic properties of the alkylferrocenium salts of tetracyanoquinodimethane (TCNQ)-type acceptors have been investigated using 1,1′-dimethyl-, 1,1′-diethyl-, 1,1′-diisopropyl-, tert-butyl-, and tert-pentyl-ferrocene as the donors. In all of the resulting salts, the donors and acceptors were stacked to form independent columns. The F4TCNQ salts had a D/A ratio of 1:1 and existed as hexagonal assembled structures composed of anion columns surrounded by cation columns. The F2TCNQ and TCNQ salts had a D/A ratio of 1:2 and existed as a rectangular arrangement of cation columns. Weak antiferromagnetic interactions were found to operate between the cations in these salts.

crystal growth and design

Crystal Architectures and Magnetic Properties of Alkylferrocenium Salts with FnTCNQ (n = 0, 2, 4): Effect of Substituents on the Self-Assembled Structures