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The enantioselective C-H alkylation of 8-ethylquinolines with enones or acrolein using a Rh III catalyst and a chiral carboxylic acid is described. Under mild reaction conditions, a binaphthyl-based chiral carboxylic acid enables the enantioselective cleavage of the 8-ethylquinoline C(sp 3 )-H bond. The obtained results demonstrate the utility of the combination of a high-valent group 9 metal catalyst and a chiral carboxylic acid for the enantioselective C(sp 3 )-H activation and the subsequent C-C bond formation.

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Rhodium(III)/Chiral Carboxylic Acid Catalyzed Enantioselective C(sp<sup>3</sup>)–H Alkylation of 8-Ethylquinolines with α,β-Unsaturated Carbonyl Compounds

Rhodium(III)/Chiral Carboxylic Acid Catalyzed Enantioselective C(sp3)–H Alkylation of 8-Ethylquinolines with α,β-Unsaturated Carbonyl Compounds

Rhodium(III)/Chiral Carboxylic Acid Catalyzed Enantioselective C(sp³)–H Alkylation of 8-Ethylquinolines with α,β-Unsaturated Carbonyl Compounds