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Reaction between NiCl 2 ·6H 2 O, 2-hydroxy-4-methyl-6-phenyl-pyridine-3-amidoxime (H 2 L), benzoic acid, and M(NO 3 ) 3 ·6H 2 O (M = Gd, Y) in MeCN under basic conditions yields the complexes [Ni II  4 Gd III  5 (PhCOO) 10 (HL) 4 (HL zw ) 4 (OH) 2 (NO 3 ) 2 ]Cl·13.6MeCN·H 2 O ( 1 ·13.6MeCN·H 2 O) and [Ni II  4 Y III  5 (PhCOO) 10 (HL) 4 (HL zw ) 4 (OH) 2 (NO 3 ) 1.5 (H 2 O) 0.5 ]0.5Cl(NO 3 )·3H 2 O ( 2 ·3H 2 O). Both clusters display similar structures, consisting of a bell-shaped {Ni II  4 M III  5 } unit, in which a linear "zigzag" {Ni 4 } subunit bisects the central {M III  5 } "ring". Direct (dc) and alternating current (ac) magnetic susceptibility measurements carried out in the 2-300 K temperature range for complexes 1 and 2 revealed ferromagnetic intermolecular interactions, while heat-capacity measurements for the Gd analogue suggest that complex 1 lowers its temperature from T = 9.6 K down to 2.3 K by adiabatically demagnetizing from B   i  = 7 T to B   f  = 0.

A Ferromagnetically Coupled, Bell-Shaped [Ni4Gd5] Cage

A Ferromagnetically Coupled, Bell-Shaped [Ni₄Gd₅] Cage