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A new series of tridentate N-8-quinolyl-salicylaldimine ligands, Hqsal-5,7-X2 [X = Cl(1), Br(2), I(3)], halo-substituted at the 5,7 position of the aminoquinoline moiety and their corresponding complexes with FeIII were synthesized and formulated as [Fe(qsal-5,7-X2)(NCS)(MeO)]2·solv. (X = Cl (1a), Br (2a), I (3a, solv = 1/2MeOH), [Fe4(qsal-5,7-X2)4(NCS)2(MeO)2]·solv. (X = Br (2b), I (3b; solv = 4CH2Cl2)) by single-crystal X-ray diffraction analysis. 1a and 2a are isostructural dimers where each FeIII metal ion, showing a distorted octahedral environment, is bound by a N,N,O tridentate (qsal-5,7-X2)− (X = Cl and Br) ligand, a N-coordinated SCN– anion, and a bridging methanolate anion. 2b and 3b are centrosymmetric tetramers where each FeIII is bound by three nitrogen atoms and three oxygen atoms derived from a tridentate (qsal-5,7-X2)− (X = Br and I), a SCN–, a bridging methanolate anion, and a bridging μ2-oxy moiety. In 3b, the iodine atoms dominate the packing interactions through the establishment of a ...

crystal growth and design

Structural Diversity in a New Series of Halogenated Quinolyl Salicylaldimides-Based Fe<sup>III</sup> Complexes Showing Solid-State Halogen-Bonding/Halogen···Halogen Interactions

Structural Diversity in a New Series of Halogenated Quinolyl Salicylaldimides-Based FeIII Complexes Showing Solid-State Halogen-Bonding/Halogen···Halogen Interactions

Structural Diversity in a New Series of Halogenated Quinolyl Salicylaldimides-Based Fe^III Complexes Showing Solid-State Halogen-Bonding/Halogen···Halogen Interactions