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The formation and structural properties of solid solutions containing 3-chloro-trans-cinnamic acid (3-ClCA) and 3-bromo-trans-cinnamic acid (3-BrCA) are explored across a range of compositions. Two distinct γ-type structures of 3-ClCA/3-BrCA solid solutions and two distinct β-type structures of 3-ClCA/3-BrCA solid solutions are reported and structurally characterized. One of the γ-type structures is isostructural with the known γ polymorphs of pure 3-ClCA and pure 3-BrCA, whereas the other γ-type structure has not been observed previously for either pure 3-ClCA or pure 3-BrCA (representing a rare case in which the structure of the solid solution is not known for the pure phases of either of the constituent molecules). One of the β-type structures of the 3-ClCA/3-BrCA solid solutions is similar to the β polymorph of pure 3-ClCA, whereas the other β-type structure is similar to the β polymorph of pure 3-BrCA. The specific β-type structure formed is found to depend on the relative amounts of 3-BrCA and 3-ClC...

Structural Diversity of Solid Solutions Formed between 3-Chloro-trans-cinnamic acid and 3-Bromo-trans-cinnamic Acid