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LBL-1249 A general radio-gas-chromatographic analysis system has been developed for hydrogen and c1 to c7 alkanes and alkenes. Peaks were monitored at a constant flow rate in the same detector (a beta proportional counter) and the injection volume was large. A system of four columns used in series gave adequate resolution of more than twenty products from the whole sample. This system was a combination of: (1) stop-flow, (2) recycle, (3) center-cut, (4) stepwise temperature programming and (5) stepwise pressure programming techniques.

Multicolumn radio-gas chromatographic analysis of recoil tritium reaction products