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We report on the structural properties of epitaxial FeO layers grown bymolecular beam epitaxy on MgO(111). The successful stabilization of polar FeOfilms as thick as 16 monolayers (ML), obtained by deposition and subsequentoxidation of single Fe layers, is presented. FeO/MgO(111) thin films werechemically and structurally characterized using low-energy electrondiffraction, Auger electron spectroscopy and conversion electron Mossbauerspectroscopy (CEMS). Detailed in situ CEMS measurements as a function of thefilm thickness demonstrated a size-effect-induced evolution of the hyperfineparameters, with the thickest film exhibiting the bulk-wustite hyperfinepattern. Ex situ CEMS investigation confirmed the magnetic ordering of thewustite thin film phase at liquid nitrogen temperature.

Layer-by-layer epitaxial growth of polar FeO(111) thin films on MgO(111)