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A novel design has been proposed for a facile and rapid build-up of highlytailorable nanostructured multishells on metal oxide particles(graphene/TiOx@TiO2) under a dry inert atmosphere to maximize the visible-lightphotocatalytic performance. We also thoroughly and systematically investigatedthe as-prepared nanostructured particle surface and the mechanisms of theextraordinary in-situ graphene growth on the TiOx@TiO2 nanoparticles achievedby a rapid-concomitant reaction in the metal oxide (TiO2)/polymer (polymethylmethacrylate) interface under microwave irradiation. The as-prepared compositematerials are also found to perform a better photocatalytic activity incomparison to the traditional synthesis pathway for degradation of organicpollutants under visible light, associated with the synergetic effects ofhomo-/hetero-junction on TiO2.

Single nanosized graphene/TiOx multi-shells on TiO2 core via rapid-concomitant reaction pathway on metal oxide/polymer interface