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An experimental approach in conducting NMR measurements at supercriticalparameters of state is discussed. A novel design of the high-pressure NMR cellwas developed which allowed eliminating the field inhomogeneity and, thus,increasing the sensitivity of the experiment at the supercritical state.Analysis of the MD simulations and NMR data showed that two conformers ofibuprofen dominate in the solution in supercritical CO2 along the criticalisochore 1.3 \r{ho}cr(CO2). Conformer populations calculated from MDsimulations and from NMR spectra agree with each other

High-pressure NMR spectroscopy in studies of the conformational composition of small molecules of ibuprofen in supercritical carbon dioxide